Baltus, Christine, Press, Neil J., Antonijevic, Milan D. ORCID: https://orcid.org/0000-0002-5847-7886, Tizzard, Graham J., Coles, Simon J. and Spencer, John (2012) Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state. Tetrahedron, 68 (45). pp. 9272-9277. ISSN 0040-4020 (doi:10.1016/j.tet.2012.08.062)

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Abstract

A biphenyl library incorporating amide and sulfonamide groups has been synthesised via microwave-mediated Suzuki–Miyaura couplings. Many derivatives were crystallised from dichloromethane/methanol and analysed by single crystal X-ray diffraction. An interesting structure was obtained for N-(4′-methylbiphenyl-4-yl)acetamide with Z′=6 and hydrogen-bonding networks of the type N–H…O in the unit cell.

Item Type:	Article
Uncontrolled Keywords:	cross coupling, microwaves, biphenylamides, hydrogen bonds, Z', X-ray crystallography
Subjects:	Q Science > QD Chemistry
Faculty / School / Research Centre / Research Group:	Faculty of Engineering & Science Faculty of Engineering & Science > School of Science (SCI)
Related URLs:	Publisher
Last Modified:	15 Nov 2021 17:01
URI:	http://gala.gre.ac.uk/id/eprint/10520

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