Skip navigation

Supporting‐electrolyte‐free electrochemical methoxymethylation of alcohols using a 3D‐printed electrosynthesis continuous flow cell system

Supporting‐electrolyte‐free electrochemical methoxymethylation of alcohols using a 3D‐printed electrosynthesis continuous flow cell system

van Melis, Carlo G. W., Penny, Matthew R., Garcia, Anthony D., Petti, Alessia, Dobbs, Adrian P., Hilton, Stephen T. and Lam, Kevin ORCID: 0000-0003-1481-9212 (2019) Supporting‐electrolyte‐free electrochemical methoxymethylation of alcohols using a 3D‐printed electrosynthesis continuous flow cell system. ChemElectrochem, 6 (16). pp. 4144-4148. ISSN 2196-0216 (Print), 2196-0216 (Online) (doi:https://doi.org/10.1002/celc.201900815)

[img] PDF (Author's Accepted Manuscript)
24666 LAM_Electrochemical_Methoxymethylation_Flow_Cell_System_(AAM)_2019.pdf - Accepted Version
Restricted to Registered users only until 4 June 2020.

Download (577kB) | Request a copy

Abstract

We describe the development of a novel low‐cost small‐footprint 3D‐printed electrosynthesis continuous flow cell system that was designed and adapted to fit a commercially available Electrasyn 2.0. The utility and effectiveness of the combined flow/electrochemistry system over the batch process was demonstrated in the development of an improved and supporting‐electrolyte‐free version of our anodic methoxymethylation of alcohols.

Item Type: Article
Uncontrolled Keywords: green chemistry, electrosynthesis, MOM ether, flow chemistry, flow electrochemistry, 3D printing
Subjects: Q Science > QD Chemistry
Faculty / Department / Research Group: Faculty of Engineering & Science
Faculty of Engineering & Science > Department of Pharmaceutical, Chemical & Environmental Sciences
Last Modified: 30 Aug 2019 12:53
Selected for GREAT 2016: None
Selected for GREAT 2017: None
Selected for GREAT 2018: None
Selected for GREAT 2019: GREAT 6
URI: http://gala.gre.ac.uk/id/eprint/24666

Actions (login required)

View Item View Item

Downloads

Downloads per month over past year

View more statistics