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Supporting‐electrolyte‐free electrochemical methoxymethylation of alcohols using a 3D‐printed electrosynthesis continuous flow cell system

Supporting‐electrolyte‐free electrochemical methoxymethylation of alcohols using a 3D‐printed electrosynthesis continuous flow cell system

van Melis, Carlo G. W., Penny, Matthew R., Garcia, Anthony D., Petti, Alessia, Dobbs, Adrian P. ORCID: 0000-0002-7241-7118, Hilton, Stephen T. and Lam, Kevin ORCID: 0000-0003-1481-9212 (2019) Supporting‐electrolyte‐free electrochemical methoxymethylation of alcohols using a 3D‐printed electrosynthesis continuous flow cell system. ChemElectrochem, 6 (16). pp. 4144-4148. ISSN 2196-0216 (Print), 2196-0216 (Online) (doi:https://doi.org/10.1002/celc.201900815)

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Abstract

We describe the development of a novel low‐cost small‐footprint 3D‐printed electrosynthesis continuous flow cell system that was designed and adapted to fit a commercially available Electrasyn 2.0. The utility and effectiveness of the combined flow/electrochemistry system over the batch process was demonstrated in the development of an improved and supporting‐electrolyte‐free version of our anodic methoxymethylation of alcohols.

Item Type: Article
Uncontrolled Keywords: green chemistry, electrosynthesis, MOM ether, flow chemistry, flow electrochemistry, 3D printing
Subjects: Q Science > QD Chemistry
Faculty / School / Research Centre / Research Group: Faculty of Engineering & Science
Faculty of Engineering & Science > School of Science (SCI)
Last Modified: 21 Oct 2020 22:31
URI: http://gala.gre.ac.uk/id/eprint/24666

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