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Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state

Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state

Baltus, Christine, Press, Neil J., Antonijevic, Milan D., Tizzard, Graham J., Coles, Simon J. and Spencer, John (2012) Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state. Tetrahedron, 68 (45). pp. 9272-9277. ISSN 0040-4020 (doi:10.1016/j.tet.2012.08.062)

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Abstract

A biphenyl library incorporating amide and sulfonamide groups has been synthesised via microwave-mediated Suzuki–Miyaura couplings. Many derivatives were crystallised from dichloromethane/methanol and analysed by single crystal X-ray diffraction. An interesting structure was obtained for N-(4′-methylbiphenyl-4-yl)acetamide with Z′=6 and hydrogen-bonding networks of the type N–H…O in the unit cell.

Item Type: Article
Uncontrolled Keywords: cross coupling, microwaves, biphenylamides, hydrogen bonds, Z', X-ray crystallography
Subjects: Q Science > QD Chemistry
Faculty / Department / Research Group: Faculty of Engineering & Science > Department of Pharmaceutical, Chemical & Environmental Sciences
Related URLs:
Last Modified: 17 Oct 2016 09:12
Selected for GREAT 2016: None
Selected for GREAT 2017: None
Selected for GREAT 2018: None
URI: http://gala.gre.ac.uk/id/eprint/10520

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