Skip navigation

Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state

Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state

Baltus, Christine, Press, Neil J., Antonijevic, Milan D. ORCID: 0000-0002-5847-7886, Tizzard, Graham J., Coles, Simon J. and Spencer, John (2012) Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state. Tetrahedron, 68 (45). pp. 9272-9277. ISSN 0040-4020 (doi:10.1016/j.tet.2012.08.062)

Full text not available from this repository.

Abstract

A biphenyl library incorporating amide and sulfonamide groups has been synthesised via microwave-mediated Suzuki–Miyaura couplings. Many derivatives were crystallised from dichloromethane/methanol and analysed by single crystal X-ray diffraction. An interesting structure was obtained for N-(4′-methylbiphenyl-4-yl)acetamide with Z′=6 and hydrogen-bonding networks of the type N–H…O in the unit cell.

Item Type: Article
Uncontrolled Keywords: cross coupling, microwaves, biphenylamides, hydrogen bonds, Z', X-ray crystallography
Subjects: Q Science > QD Chemistry
Faculty / Department / Research Group: Faculty of Engineering & Science > Department of Pharmaceutical, Chemical & Environmental Sciences
Related URLs:
Last Modified: 17 Oct 2016 09:12
Selected for GREAT 2016: None
Selected for GREAT 2017: None
Selected for GREAT 2018: None
URI: http://gala.gre.ac.uk/id/eprint/10520

Actions (login required)

View Item View Item